MARINE
ALKALOIDS
The study of the structures
of plant alkaloids dates back to the very beginnings of Organic
Chemistry - quinine was isolated in pure form in 1817 and morphine
10 years before that.
Oceans
cover 70% of the earth's surface and contain 95% of the biosphere.
More than 95% of all animals are invertebrates.
The
marine environment has given rise to unique biological and chemical
evolution, very different from land-based life.
Over the last quarter of a century
it has been possible to study nitrogenous substances isolated
from marine animals - we can call them 'marine alkaloids'. Just
as the interest in quinine and morphine was encouraged by the
use of such substances in medicine, so it has been shown that
many marine alkaloids have biological properties which may prove
to be of value to mankind.
Invertebrates such as sponges, soft
corals, molluscs, coelenterates, and ascidians produce secondary
metabolites of unprecedented structures; sponges and ascidians,
in particular, produce nitrogen-containing substances.
Most natural products from the oceans
are structurally novel and in addition, many possess potent biological
activities. Full biological evaluations of such substances are
however severely hampered by the difficulty of obtaining substantial
quantities - it is difficult, and indeed ecologically undesirable,
to harvest large quantities of the marine creatures from which
they are isolated; it is also difficult to grow such animals in
the laboratory.
Access to substantial quantities of
these novel substances must then be by way of chemical synthesis,
which also has the very considerable additional advantage that
it, and only it allows analogues to be prepared and thus desirable
biological activities to be maximised and any undesirable side-effects
minimised - the natural substance is, in the jargon of pharmaceutical
industry, a 'lead compound'.
We have been engaged for some time
on the development of synthetic routes to several classes of marine
alkaloids, including pyrrolo[4,3,2-de]quinolines, pyrido[3´,2´:4,5]pyrrolo[1,2-c]pyrimidines,
pyrrolo [2,3,4-kl] acridines, and pyrido[2,3,4-kl]acridines.
In some of this work we collaborate with the group of Dr. Mercedes
Alvarez in the Laboratori de Química Orgànica, Facultat
de Farmàcia, University of Barcelona, Spain, facilitated
by exchanges of personnel in both Northerly and Southerly directions.